dc.contributor.author | Savinykh, D.O | |
dc.contributor.author | Khaynakov, Sergiy | |
dc.contributor.author | Boldin, M.S. | |
dc.contributor.author | Orlova, A.I. | |
dc.contributor.author | Aleksandrov, A.A. | |
dc.contributor.author | Lantsev, E.A. | |
dc.contributor.author | Sakharov, N.V. | |
dc.contributor.author | Murashov, A.A. | |
dc.contributor.author | García-Granda, Santiago | |
dc.contributor.author | Nokhrin, A.V. | |
dc.contributor.author | Chuvil'deev, V.N. | |
dc.date.accessioned | 2019-04-01T10:19:44Z | |
dc.date.available | 2019-04-01T10:19:44Z | |
dc.date.issued | 2018 | |
dc.identifier.citation | Inorganic Materials, 54(12), p. 1267-1273 (2018); doi:10.1134/S0020168518120154 | |
dc.identifier.issn | 0020-1685 | |
dc.identifier.uri | http://hdl.handle.net/10651/50920 | |
dc.description.abstract | Ca0.75+0.5xZr1.5Fe0.5(PO4)3–x(SiO4)x (x = 0–0.5) solid solutions have been synthesized by a sol–gel process and characterized by X-ray diffraction, IR spectroscopy, and differential scanning calorimetry. As expected, the synthesized phosphatosilicates crystallize in a NaZr2(PO4)3-type structure (trigonal symmetry, sp. gr. R c). The thermal expansion of the solid solutions has been studied by high-temperature X-ray diffraction in the temperature range from 25 to 800°C. Their thermal expansion parameters have been calculated and analyzed as functions of composition. High-density ceramics based on the Ca0.875Zr1.5Fe0.5(PO4)2.75(SiO4)0.25 phosphatosilicate have been produced by spark plasma sintering and their structure and properties have been studied in detail. | spa |
dc.format.extent | p. 1267-1273 | spa |
dc.language.iso | eng | spa |
dc.relation.ispartof | Inorganic Materials, 54 | spa |
dc.rights | © Pleiades Publishing, Inc. 2018 | |
dc.rights | CC Reconocimiento - No comercial - Sin obras derivadas 4.0 Internacional | |
dc.rights.uri | http://creativecommons.org/licenses/by-nc-nd/4.0/ | |
dc.title | Preparation of NZP-type Ca0.75+0.5xZr1.5Fe0.5(PO4)3-x(SiO4)x powders and ceramic, thermal expansion behavior | spa |
dc.type | journal article | spa |
dc.identifier.doi | 10.1134/S0020168518120154 | |
dc.relation.publisherversion | https://doi.org/10.1134/S0020168518120154 | |
dc.rights.accessRights | open access | spa |
dc.type.hasVersion | AM | |